Green Nanomaterials. Siddharth Patwardhan

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3.2 Microscopy

       3.2.1 Optical microscopy

       3.2.2 Electron microscopy

       3.2.3 Scanning electron microscopy

       3.2.4 Transmission electron microscopy

       3.2.5 Atomic force microscopy

       3.3 Spectroscopy applied to nanomaterials

       3.3.1 Mass spectrometry

       3.3.2 Infra-red spectroscopy

       3.3.3 X-ray photoelectron spectroscopy

       3.4 Diffraction and scattering techniques

       3.4.1 X-ray diffraction (XRD)

       3.4.2 Dynamic light scattering

       3.4.3 Small angle scattering

       3.5 Porosimetry

       3.6 Summary: key lessons for characterisation of nanomaterials

       References

       4 Conventional methods to prepare nanomaterials

       4.1 Top-down and bottom-up methods

       4.2 Top-down methods

       4.3 Bottom-up methods

       4.4 Nucleation and growth theory

       4.4.1 Homogeneous nucleation

       4.4.2 Heterogeneous nucleation

       4.4.3 Growth

       4.5 Conventional bottom-up methods

       4.5.1 Vapour-phase method

       4.5.2 Solution processing

       4.5.3 Spray conversion

       4.5.4 Sol–gel method

       4.6 Emerging bottom-up methods

       4.6.1 Principles and overview

       4.6.2 Soft lithography

       4.6.3 Dip-pen nanolithography

       4.6.4 Layer-by-layer self-assembly

       4.6.5 Solution synthesis of nanoparticles

       4.6.6 Templated synthesis

       4.7 Summary: key lessons about conventional routes to nanomaterials

       References

       Section III From biominerals to green nanomaterials

       5 Green chemistry for nanomaterials

       5.1 Sustainability of nanomaterials production

       5.2 Reasons behind unsustainability

       5.3 Evaluation of sustainability for selected methods

       5.3.1 E-factors for solution methods

       5.3.2 How green is soft lithography?

       5.3.3 Templated synthesis: surely sustainable?

       5.4 Adopting green chemistry for nanomaterials

       5.5 Biological and biochemical terminology and methods

       5.5.1 Molecular biology component

       5.5.2 Molecular biological techniques

       5.6 Summary: key lessons about sustainability nanomaterials production

       References

       6 Biomineralisation: how Nature makes nanomaterials

       6.1 Introduction

       6.2 Properties and function of biomineral types

       6.2.1 Bio-calcium phosphate (hydroxyapatite): mechanical/structural support, motion, cutting/grinding

      

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