Henley's Twentieth Century Formulas, Recipes and Processes. Various
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To Make Wood Acid- and Chlorine-proof.
—Take 6 pounds of wood tar and 12 pounds rosin, and melt them together in an iron kettle, after which stir in 8 pounds finely powdered brick dust. The damaged parts must be cleaned perfectly and dried, whereupon they may be painted over with the warm preparation or filled up and drawn off, leaving the film on the inside.
Protecting Cement Against Acid.
—A paint to protect cement against acid is obtained by mixing pure asbestos, very finely powdered, with a thick solution of {10} sodium silicate. The sodium silicate must be as alkaline as possible. The asbestos is first rubbed with a small quantity of the silicate, until a cake is obtained and then kept in well-closed vessels. For use this cake is simply thinned with a solution of the silicate, which furnishes a paint two or three applications of which protect the walls of reservoirs, etc., against any acid solid or liquid. This mass may also be employed for making a coating of sandstone.
To Make Corks Impermeable And Acid-proof.
—Choose your corks carefully. Then plunge them into a solution of gelatin or common glue, 15 parts, in 24 parts of glycerine and 500 parts of water, heated to 44° or 48° C. (112°–120° F.), and keep them there for several hours. On removing the corks, which should be weighted down in the solution, dry them in the shade until they are free from all surplus moisture. They are now perfectly tight, retaining at the same time the greater portion of their elasticity and suppleness. To render them acid-proof, they should be treated with a mixture of vaseline, 2 parts, and paraffine 7 parts, heated to about 105° F. This second operation may be avoided by adding to the gelatin solution a little ammonium dichromate and afterwards exposing the corks to the light.
Lining For Acid Receptacles.
—Plates are formed of 1 part of brown slate, 2 of powdered glass, and 1 of Portland cement, the whole worked up with silicate of soda, molded and dried. Make a cement composed of ground slate and silicate of soda and smear the surface for the lining; then, while it is still plastic, apply the plates prepared as above described. Instead of these plates, slabs of glass or porcelain or similar substances may be employed with the same cement.
ACACIA, MUCILAGE OF: See Adhesives under Mucilages.
ACID-PROOF GLASS: See Glass.
ACID-RESISTING PAINT: See Paint.
ACIDS, SOLDERING: See Solders.
ACID STAINS FROM THE SKIN, TO REMOVE: See Cleaning Preparations and Methods.
ACID TEST FOR VINEGAR: See Vinegar.
ADHESIVES
Glues:
Manufacture Of Glue.
—I.—The usual process of removing the phosphate of lime from bones for glue-making purposes by means of dilute hydrochloric acid has the disadvantage that the acid cannot be regenerated. Attempts to use sulphurous acid instead have so far proved unsuccessful, as, even with the large quantities used, the process is very slow. According to a German invention this difficulty with sulphurous acid can be avoided by using it in aqueous solution under pressure. The solution of the lime goes on very rapidly, it is claimed, and no troublesome precipitation of calcium sulphite takes place. Both phosphate of lime and sulphurous acid are regenerated from the lyes by simple distillation.
II.—Bones may be treated with successive quantities of combined sulphurous acid and water, from which the heat of combination has been previously dissipated, the solution being removed after each treatment, before the bone salts dissolved therein precipitate, and before the temperature rises above 74° F.—U. S. Pat. 783,784.
III.—A patent relating to the process for treating animal sinews, preparatory for the glue factory, has been granted to Florsheim, Chicago, and consists in immersing animal sinews successively in petroleum or benzine to remove the outer fleshy animal skin; in a hardening or preserving bath, as boric acid, or alum or copper sulphate; and in an alkaline bath to remove fatty matter from the fibrous part of the sinews. The sinews are afterwards tanned and disintegrated.
Test For Glue.
—The more water the glue takes up, swelling it, the better it is. Four ounces of the glue to be examined are soaked for about 12 hours in a cool place in 4 pounds of cold water. If the glue has dissolved after this time, it is of bad quality and of little value; but if it is coherent, gelatinous, and weighing double, it is good; if it weighs up to 16 ounces, it is very good; if as much as 20 ounces, it may be called excellent.
To Prevent Glue From Cracking.
—To prevent glue from cracking, which frequently occurs when glued articles are {11} exposed to the heat of a stove, a little chloride of potassium is added. This prevents the glue from becoming dry enough to crack. Glue thus treated will adhere to glass, metals, etc., and may also be used for pasting on labels.
Preventing The Putrefaction Of Strong Glues.
—The fatty matter always existing in small quantity in sheets of ordinary glue affects the adhesive properties and facilitates the development of bacteria, and consequently putrefaction and decomposition. These inconveniences are remedied by adding a small quantity of caustic soda to the dissolved glue. The soda prevents decomposition absolutely; with the fatty matter it forms a hard soap which renders it harmless.
Liquid Glues.—
I.— | Glue | 3 ounces |
---|---|---|
Gelatin | 3 ounces | |
Acetic acid | 4 ounces | |
Water | 2 ounces | |
Alum | 30 grains | |
Heat together for 6 hours, skim, and add: | ||
II.— | Alcohol | 1 fluid ounce |
Brown glue, No. 2. | 2 pounds | |
Sodium carbonate | 11 ounces | |
Water | 3 1/2 pints | |
Oil of clove | 160 minims |
Dissolve the soda in the water, pour the solution over the dry glue, let stand over night or till thoroughly soaked and swelled, then heat carefully on a water bath until dissolved. When nearly cold stir in the oil of cloves.
By using white glue, a finer article, fit for fancy work, may be made.
III.—Dissolve by heating 60 parts of borax in 420 parts of water, add 480 parts dextrin (pale yellow) and 50 parts of glucose and heat carefully with continued stirring, to complete solution; replace the evaporated water and pour through flannel.
The glue made in this way remains clear quite a long time, and possesses great adhesive power; it also dries very quickly, but upon careless and extended heating above 90° C. (194° F.), it is apt to turn brown and brittle.
IV.—Pour 50 parts of warm (not hot) water over 50 parts of Cologne glue and allow to soak over night. Next day the swelled glue is dissolved with moderate heat, and if still too thick, a little